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The draw left champions Barca top on 36 points after 17 games with Real also on 36, five clear of third-placed Sevilla.
Title-holders Liverpool will face Diego Simeone's Atletico Madrid.
The draw leaves Barca still leading with 35 points from 16 games but Real Madrid, on 34, can take their place at the top if they win at Valencia on Sunday.
On a good night for English clubs, Wolverhampton Wanderers thrashed Besiktas 4-0 in Group K, while Arsenal came from two goals down to draw 2-2 away to Standard Liege and finish first in their pool ahead of Eintracht Frankfurt.
The victory means Zinedine Zidane's side move to the top of the table, for a few hours at least, before Barcelona play later on Saturday at home to Real Mallorca.
Emery's final match in charge was Thursday's 2-1 Europa League home defeat to German side Eintracht Frankfurt which extended their winless run in all competitions to seven games, the worst streak since February 1992 under George Graham.
La Liga champions Barcelona's long winning streak came to an abrupt halt when they suffered a shock 3-1 defeat away to Levante on Saturday.
Real were full of confidence after hammering Leganes 5-0 in mid-week for their biggest win of a stop-start season and appeared to get off to a great start when Eden Hazard struck early. But the goal was ruled out for offside after a VAR review.
Manchester United claimed their first away win in any competition since March as they beat Partizan Belgrade 1-0, but AS Roma were held to a 1-1 draw as Borussia Moenchengladbach equalised deep into stoppage time.
The back-to-back failures have forced the franchise’s management to bring back Spanish coach Antonio Lopez Habas, who guided them to victory in the league’s inaugural edition.