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Villarreal goalkeeper Geronimo Rulli kept his composure to score in a nerve-shredding, seemingly never-ending shootout then denied David de Gea as his side won their first major trophy by beating Manchester United 11-10 on penalties.
United's defeat means City are 10 points clear with both sides having three games left to play.
Fans stormed the stadium and pitch before kick-off in protest against the club's owners - the Glazer family.
Debutant director Mustafa Gutz can certainly take pride in making such an entertaining movie on a big canvas, that too, with a cast of around one hundred new comers.
United edged their heavyweight tie with AC Milan as Paul Pogba came off the bench to score the goal that secured a 1-0 win in the San Siro for a 2-1 aggregate triumph.
Borussia Dortmund striker Erling Haaland struck in each half as they advanced to the quarterfinals after a 2-2 draw with Sevilla in their last-16 second leg to complete a 5-4 aggregate win.
United won thanks to an early penalty from Bruno Fernandes and a second-half strike from Luke Shaw with the result narrowing City's lead at the top of the table to 11 points over United with 10 games remaining.
United became only the second team to win a Premier League game 9-0, matching their 9-0 win over Ipswich Town in 1995 and also Leicester City's away rout of Southampton in 2019.
Manchester United were held to a 2-2 draw at Leicester City while Manchester City climbed to fifth thanks to a 2-0 win over Newcastle United.
The results leave Tottenham Hotspur top of the table on 24 points level with Liverpool.